庞勇;曾岗;
1:河南公安高等专科学校
2:哈尔滨工业大学材料科学与工程学院
摘要:采用电子束物理气相沉积(EB-PVD)工艺制备了NiCrAl高温合金薄板。采用XRD对薄板进行了相分析,结果表明,这种高温合金薄板是由γ′和γ两相组成。从薄板的横截面显微组织分析表明,高温合金中γ′以颗粒状形式弥散分布在γ基体上;从薄板的纵截面可以看出,组织为柱状晶和粒状晶交替组织。薄板的常温抗拉强度为446.89MPa。较低的抗拉强度是由于其组织不均匀并且含有柱状晶组织,柱状晶的组织各向异性,拉伸方向不是最佳受力方向。
关键词: 电子束物理气相沉积(EB-PVD);;薄板;;NiCrAl合金
Abstract: The microstructures of
as-deposited NiCrAl alloy freestanding sheet by a electron beam-physical vapor
deposition(EB-PVD)method were investigated by means of X-ray
diffractometry,Scanning Electron Microscopy and Optical Microscopy.The results
showed that the superalloy component exists mainly in γ and γ′phases.And γ′phase was dispersed in the γ matrix from the cross-sectional micrographs of as-deposited NiCrAl
superalloy sheet by EB-PVD.At the same time,it can be observed that the
equiaxed grain and columnar grain were grown by turn form the vertical-section
micrography of the sheet.The tensile strength was only 446.89MPa at room
temperature,due to the structural non-homogeneous and the presence of columnar
grains.
Keywords: Electron Beam-Physical Vapor
Deposition(EB-PVD);Sheet;NiCrAl Alloy
基金项目: 国家自然科学基金委员会资助(资助号:90205034)
参考文献:
[1]R.G.Rowe,D.W.Skelly,M.Larsen,J.Heathcote,G.R.Odette
and G.E.Lucas.Microlaminated High TemperatureIntermetallic Composites.Scripta
MetallurgicaetMaterialia.31(11)(1994)1487.
[2]金雪松,徐惠彬,宫声凯.Fe/Cu纳米多层材料的电导行为.中国科学E辑.(5)(2000)385.
[3]金雪松,毕晓日方,欧盛荃,宫声凯,徐惠彬.K18/Mo纳米多层材料的力学性能及高温稳定性.金属学报.(1)(2000).
[4]黄斌,石原庆一,新官秀夫等,重复压轧制法制备纳米级金属多层材料,金属学报,34(1998)455-458.
[5]J.Bamas,G.Palasantzas,Interface
roughness effects in thegiant magnetoresistance in magnetic
multiayers,J.Appl.Phys.,852(1991)3950-3956.
[6]H.B.Xu,S.K.Gong,L.Deng,Preparation of
thermal barriercoating for gasturbine blades by EB-PVD,Thin Solid
Films,334(1998)98-102.
[7]B.A.Movchan,EB-PVD technology in the gas
turbine in-dustry:present and future,JOM.Nov,48(1996)40-45.
[8]陈国良,林均品.有序金属间化合物结构材料,冶金工业出版社,212-230.
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